Information card for entry 4326956

Structure parameters

• Formula: C14 H35 B Co F4 N P4
• Calculated formula: C14 H35 B Co F4 N P4
• SMILES: [Co]12([N]#CC)([P](C)(C)CC[P]1(C)C)[P](C)(C)CC[P]2(C)C.[B](F)(F)(F)[F-]
• Title of publication: Synthesis and Hydride Transfer Reactions of Cobalt and Nickel Hydride Complexes to BX3 Compounds
• Authors of publication: Michael T. Mock; Robert G. Potter; Molly J. O'Hagan; Donald M. Camaioni; William G. Dougherty; W. Scott Kassel; Daniel L. DuBois
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11914 - 11928
• a: 12.4445 ± 0.0003 Å
• b: 9.1456 ± 0.0002 Å
• c: 20.0098 ± 0.0004 Å
• α: 90°
• β: 97.582 ± 0.001°
• γ: 90°
• Cell volume: 2257.45 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0308
• Residual factor for significantly intense reflections: 0.0295
• Weighted residual factors for significantly intense reflections: 0.0802
• Weighted residual factors for all reflections included in the refinement: 0.0811
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No