Information card for entry 4326959

Structure parameters

• Formula: C72 H96 B2 Co2 F8 P8
• Calculated formula: C72 H96 B2 Co2 F8 P8
• Title of publication: Synthesis and Hydride Transfer Reactions of Cobalt and Nickel Hydride Complexes to BX3 Compounds
• Authors of publication: Michael T. Mock; Robert G. Potter; Molly J. O'Hagan; Donald M. Camaioni; William G. Dougherty; W. Scott Kassel; Daniel L. DuBois
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 11914 - 11928
• a: 10.4373 ± 0.0013 Å
• b: 17.858 ± 0.002 Å
• c: 20.266 ± 0.003 Å
• α: 74.868 ± 0.006°
• β: 82.2 ± 0.005°
• γ: 84.762 ± 0.005°
• Cell volume: 3606.5 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1093
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.1873
• Weighted residual factors for all reflections included in the refinement: 0.224
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No