Information card for entry 4327059

Structure parameters

• Formula: C37 H69 Al Li N2 O2
• Calculated formula: C37 H69 Al Li N2 O2
• Title of publication: Structurally Powered Synergic 2,2,6,6-Tetramethylpiperidine Bimetallics: New Reflections through Lithium-Mediated Ortho Aluminations
• Authors of publication: Robert E. Mulvey; David R. Armstrong; Ben Conway; Elaine Crosbie; Alan R. Kennedy; Stuart D. Robertson
• Journal of publication: Inorganic Chemistry
• Year of publication: 2011
• Journal volume: 50
• Pages of publication: 12241 - 12251
• a: 11.4941 ± 0.0002 Å
• b: 19.1867 ± 0.0003 Å
• c: 17.9794 ± 0.0004 Å
• α: 90°
• β: 106.101 ± 0.002°
• γ: 90°
• Cell volume: 3809.53 ± 0.13 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0628
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.1027
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No