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Information card for entry 4327061
Preview
Coordinates | 4327061.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H54 Al Li N2 O |
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Calculated formula | C24 H54 Al Li N2 O |
SMILES | [Li]1([O]2CCCC2)[N](C(C)C)(C(C)C)[Al]([N]1(C(C)C)C(C)C)(CC(C)C)CC(C)C |
Title of publication | Structurally Powered Synergic 2,2,6,6-Tetramethylpiperidine Bimetallics: New Reflections through Lithium-Mediated Ortho Aluminations |
Authors of publication | Robert E. Mulvey; David R. Armstrong; Ben Conway; Elaine Crosbie; Alan R. Kennedy; Stuart D. Robertson |
Journal of publication | Inorganic Chemistry |
Year of publication | 2011 |
Journal volume | 50 |
Pages of publication | 12241 - 12251 |
a | 11.3522 ± 0.0002 Å |
b | 17.008 ± 0.0004 Å |
c | 14.0982 ± 0.0004 Å |
α | 90° |
β | 90.351 ± 0.003° |
γ | 90° |
Cell volume | 2722 ± 0.11 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0656 |
Residual factor for significantly intense reflections | 0.04 |
Weighted residual factors for significantly intense reflections | 0.0955 |
Weighted residual factors for all reflections included in the refinement | 0.1003 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.939 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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