Information card for entry 4327305

Structure parameters

• Formula: C30 H30 Gd N11 Ni2 O15
• Calculated formula: C30 H20 Gd N11 Ni2 O15
• Title of publication: Novel Heterometallic 3d-4f Metal-Azido Complex of Mixed Ligands with Unprecedented Structure Type: Synthesis, Structure, and Magnetic Properties
• Authors of publication: Fu-Chen Liu; Yong-Fei Zeng; Jiao Jiao; Jian-Rong Li; Xian-He Bu; Joan Ribas; Stuart R. Batten
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Pages of publication: 6129 - 6131
• a: 8.1859 ± 0.0009 Å
• b: 26.853 ± 0.003 Å
• c: 16.8859 ± 0.0018 Å
• α: 90°
• β: 95.351 ± 0.002°
• γ: 90°
• Cell volume: 3695.6 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0315
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.0789
• Weighted residual factors for all reflections included in the refinement: 0.0807
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No