Information card for entry 4327524

Structure parameters

• Formula: C54 H53 Al3 Cl3 N3 O3
• Calculated formula: C54 H53 Al3 Cl3 N3 O3
• Title of publication: Reactions of Amides with Organoaluminum Compounds: Factors Affecting the Coordination Mode of Aluminum Amidates
• Authors of publication: Bor-Hunn Huang; Te-Liang Yu; Yi-Lun Huang; Bao-Tsan Ko; Chu-Chieh Lin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2987 - 2994
• a: 13.2398 ± 0.0012 Å
• b: 14.0254 ± 0.0014 Å
• c: 17.0097 ± 0.0016 Å
• α: 88.242 ± 0.002°
• β: 72.244 ± 0.002°
• γ: 87.145 ± 0.002°
• Cell volume: 3004 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1211
• Residual factor for significantly intense reflections: 0.0603
• Weighted residual factors for significantly intense reflections: 0.1617
• Weighted residual factors for all reflections included in the refinement: 0.195
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No