Information card for entry 4327542

Structure parameters

• Formula: C42 H37 N O Os P2
• Calculated formula: C42 H37 N O Os P2
• SMILES: [OsH2]1([P](c2ccccc2)(c2ccccc2)c2ccccc2)([P](c2ccccc2)(c2ccccc2)c2ccccc2)Nc2ccccc2O1
• Title of publication: Structural Systematics for o-C6H4XY Ligands with X,Y= O, NH, and S Donor Atoms. o-Iminoquinone and o-Iminothioquinone Complexes of Ruthenium and Osmium
• Authors of publication: Samaresh Bhattacharya; Parna Gupta; Falguni Basuli; Cortlandt G. Pierpont
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5810 - 5816
• a: 9.2386 ± 0.0003 Å
• b: 18.414 ± 0.0006 Å
• c: 20.3305 ± 0.0007 Å
• α: 90°
• β: 97.225 ± 0.001°
• γ: 90°
• Cell volume: 3431.2 ± 0.2 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1187
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for significantly intense reflections: 0.0949
• Weighted residual factors for all reflections included in the refinement: 0.1144
• Goodness-of-fit parameter for all reflections included in the refinement: 0.953
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No