Information card for entry 4327648

Structure parameters

• Formula: C55 H86 B N2 O13 P4 Re
• Calculated formula: C55 H86 B N2 O13 P4 Re
• SMILES: [Re]([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)([NH]=Nc1ccccc1)C#[O].[B-](c1ccccc1)(c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Preparations, Structures, and Electrochemical Studies of Aryldiazene Complexes of Rhenium: Syntheses of the First Heterobinuclear and Heterotrinuclear Derivatives with Bis(diazene) or Bis(diazenido) Bridging Ligands
• Authors of publication: Gabriele Albertin; Stefano Antoniutti; Alessia Bacchi; Giovanni B. Ballico; Emilio Bordignon; Giancarlo Pelizzi; Maria Ranieri; Paolo Ugo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3265 - 3279
• a: 15.38 ± 0.005 Å
• b: 13.037 ± 0.005 Å
• c: 16.649 ± 0.005 Å
• α: 90.33 ± 0.05°
• β: 91.2 ± 0.1°
• γ: 89.71 ± 0.09°
• Cell volume: 3337 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0811
• Weighted residual factors for all reflections included in the refinement: 0.097
• Goodness-of-fit parameter for all reflections included in the refinement: 0.829
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No