Information card for entry 4328736

Structure parameters

• Formula: C108 H87 D24 N3 P6 S7 Si3 Sn4
• Calculated formula: C108 H87 D24 N3 P6 S7 Si3 Sn4
• Title of publication: Reactivity of a Tin(II) (Iminophosphinoyl)(thiophosphinoyl)methanediide Complex Toward Sulfur: Synthesis and 119Sn Mössbauer Spectroscopic Studies of [{(μ-S)SnC(PPh2=NSiMe3)(PPh2=S)}3Sn(μ3-S)]
• Authors of publication: Jia-Yi Guo; Hong-Wei Xi; Israel Nowik; Rolfe H. Herber; Yongxin Li; Kok Hwa Lim; Cheuk-Wai So
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 3996 - 4001
• a: 16.4619 ± 0.001 Å
• b: 33.693 ± 0.002 Å
• c: 19.8683 ± 0.0012 Å
• α: 90°
• β: 92.672 ± 0.004°
• γ: 90°
• Cell volume: 11008 ± 1.1 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1327
• Residual factor for significantly intense reflections: 0.077
• Weighted residual factors for significantly intense reflections: 0.1862
• Weighted residual factors for all reflections included in the refinement: 0.2238
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No