Information card for entry 4328739

Structure parameters

• Formula: C57 H58 Cl2 Ge Ir O2 P4 Rh
• Calculated formula: C57 H58 Cl2 Ge Ir O2 P4 Rh
• Title of publication: Germyl- and Germylene-Bridged Complexes of Rh/Ir and Subsequent Chemistry of a Bridging Germylene Group
• Authors of publication: Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 4020 - 4034
• a: 12.3318 ± 0.0007 Å
• b: 17.7653 ± 0.001 Å
• c: 25.2646 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5534.9 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0192
• Residual factor for significantly intense reflections: 0.0188
• Weighted residual factors for significantly intense reflections: 0.0524
• Weighted residual factors for all reflections included in the refinement: 0.0526
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No