Information card for entry 4328741

Structure parameters

• Formula: C66 H60 Cl4 Ge Ir O2 P4 Rh
• Calculated formula: C64 H56 Ge Ir O2 P4 Rh
• Title of publication: Germyl- and Germylene-Bridged Complexes of Rh/Ir and Subsequent Chemistry of a Bridging Germylene Group
• Authors of publication: Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 4020 - 4034
• a: 13.0777 ± 0.0006 Å
• b: 13.0777 ± 0.0006 Å
• c: 32.0219 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4742.9 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 144
• Hermann-Mauguin space group symbol: P 31
• Hall space group symbol: P 31
• Residual factor for all reflections: 0.0525
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1177
• Weighted residual factors for all reflections included in the refinement: 0.1179
• Goodness-of-fit parameter for all reflections included in the refinement: 1.222
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No