Information card for entry 4329230

Structure parameters

• Common name: [LNi2]_3.2DMF_0.15iPr2O
• Formula: C72.5 H70.5 N7.2 Ni2 O9.35
• Calculated formula: C72.5 H70.5 N7.33333 Ni2 O9.35
• Title of publication: Hierarchical Helix of Helix in the Crystal: Formation of Variable-Pitch Helical π-Stacked Array of Single-Helical Dinuclear Metal Complexes
• Authors of publication: Shigehisa Akine; Hiroki Nagumo; Tatsuya Nabeshima
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 5506 - 5508
• a: 22.1467 ± 0.0006 Å
• b: 27.5484 ± 0.0008 Å
• c: 31.0547 ± 0.0008 Å
• α: 90°
• β: 90.589 ± 0.001°
• γ: 90°
• Cell volume: 18945.7 ± 0.9 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.0489
• Weighted residual factors for significantly intense reflections: 0.1312
• Weighted residual factors for all reflections included in the refinement: 0.1377
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No