Information card for entry 4329467

Structure parameters

• Chemical name: tris(μ~3~-phenylselenido)-tris(μ~2~-phenylselenido)-tris(trimethylphosphine) -methyl-tetra-copper-gallium pentane solvate tetrahydrofuran solvate
• Formula: C54.5 H60 Cu4 Ga O1.5 P3 Se6
• Calculated formula: C54.49 H59.97 Cu4 Ga O1.5 P3 Se6
• Title of publication: Trialkylphosphine-Stabilized Copper(I) Gallium(III) Phenylchalcogenolate Complexes: Crystal Structures and Generation of Ternary Semiconductors by Thermolysis
• Authors of publication: Oliver Kluge; Harald Krautscheid
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 6655 - 6666
• a: 16.3325 ± 0.0007 Å
• b: 16.3325 ± 0.0007 Å
• c: 27.1616 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 6274.7 ± 0.5 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 165
• Hermann-Mauguin space group symbol: P -3 c 1
• Hall space group symbol: -P 3 2"c
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0744
• Goodness-of-fit parameter for all reflections included in the refinement: 0.97
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No