Crystallography Open Database

Information card for entry 4329829

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Coordinates	4329829.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6.91 H20.74 Cl3.09 N2 Si4
Calculated formula	C6.912 H20.736 Cl3.088 N2 Si4
Title of publication	Chlorine/Methyl Exchange Reactions in Silylated Aminostibanes: A New Route To Stibinostibonium Cations
Authors of publication	Christian Hering; Mathias Lehmann; Axel Schulz; Alexander Villinger
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	8212 - 8224
a	6.5182 ± 0.0003 Å
b	13.0335 ± 0.0006 Å
c	10.8415 ± 0.0005 Å
α	90°
β	101.686 ± 0.002°
γ	90°
Cell volume	901.95 ± 0.07 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0545
Residual factor for significantly intense reflections	0.0385
Weighted residual factors for significantly intense reflections	0.1072
Weighted residual factors for all reflections included in the refinement	0.1158
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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