Information card for entry 4329831

Structure parameters

• Formula: C30 H37 Cl2 N Sb Si
• Calculated formula: C30 H37 Cl2 N Sb Si
• Title of publication: Chlorine/Methyl Exchange Reactions in Silylated Aminostibanes: A New Route To Stibinostibonium Cations
• Authors of publication: Christian Hering; Mathias Lehmann; Axel Schulz; Alexander Villinger
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8212 - 8224
• a: 16.953 ± 0.012 Å
• b: 19.071 ± 0.013 Å
• c: 19.49 ± 0.013 Å
• α: 90.888 ± 0.019°
• β: 103.057 ± 0.017°
• γ: 97.44 ± 0.02°
• Cell volume: 6080 ± 7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0995
• Residual factor for significantly intense reflections: 0.0431
• Weighted residual factors for significantly intense reflections: 0.0922
• Weighted residual factors for all reflections included in the refinement: 0.1256
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No