Crystallography Open Database

Information card for entry 4329838

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Coordinates	4329838.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H34 Cl0.13 N6.63 Sb Si
Calculated formula	C27 H34 Cl0.125 N6.625 Sb Si
Title of publication	Chlorine/Methyl Exchange Reactions in Silylated Aminostibanes: A New Route To Stibinostibonium Cations
Authors of publication	Christian Hering; Mathias Lehmann; Axel Schulz; Alexander Villinger
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	8212 - 8224
a	10.8087 ± 0.0003 Å
b	11.6186 ± 0.0004 Å
c	12.4497 ± 0.0004 Å
α	72.464 ± 0.001°
β	71.959 ± 0.001°
γ	87.985 ± 0.001°
Cell volume	1414.59 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0298
Residual factor for significantly intense reflections	0.024
Weighted residual factors for significantly intense reflections	0.0595
Weighted residual factors for all reflections included in the refinement	0.0636
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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