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Information card for entry 4329871
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Coordinates | 4329871.cif |
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Original paper (by DOI) | HTML |
Formula | C43 H54 Ni6 O3 |
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Calculated formula | C43 H54 Ni6 O3 |
Title of publication | Triple C-H Bond Activation of a Nickel-Bound Methyl Group: Synthesis and X-Ray Structure of a Carbide Cluster (NiCp)6(μ6-C) |
Authors of publication | Włodzimierz Buchowicz; Beata Herbaczyńska; Lucjan B. Jerzykiewicz; Tadeusz Lis; Stanisław Pasynkiewicz; Antoni Pietrzykowski |
Journal of publication | Inorganic Chemistry |
Year of publication | 2012 |
Journal volume | 51 |
Pages of publication | 8292 - 8297 |
a | 15.637 ± 0.004 Å |
b | 15.637 ± 0.004 Å |
c | 9.351 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 120° |
Cell volume | 1980.1 ± 1 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 4 |
Space group number | 186 |
Hermann-Mauguin space group symbol | P 63 m c |
Hall space group symbol | P 6c -2c |
Residual factor for all reflections | 0.1273 |
Residual factor for significantly intense reflections | 0.0682 |
Weighted residual factors for significantly intense reflections | 0.1558 |
Weighted residual factors for all reflections included in the refinement | 0.1804 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.03 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4329871.html
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