Information card for entry 4329958

Structure parameters

• Formula: C62 H142 Li2 N0 O11 Si8 Sn9
• Calculated formula: C62 H142 Li2 O11 Si8 Sn9
• Title of publication: {Sn9[Si(SiMe3)3]2}2-: A Metalloid Tin Cluster Compound With a Sn9 Core of Oxidation State Zero
• Authors of publication: Claudio Schrenk; Florian Winter; Rainer Pöttgen; Andreas Schnepf
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 8583 - 8588
• a: 14.949 ± 0.003 Å
• b: 15.745 ± 0.003 Å
• c: 21.602 ± 0.004 Å
• α: 90°
• β: 104.93 ± 0.03°
• γ: 90°
• Cell volume: 4912.9 ± 1.8 ų
• Cell temperature: 149 ± 2 K
• Ambient diffraction temperature: 149 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0999
• Weighted residual factors for all reflections included in the refinement: 0.1023
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No