Information card for entry 4330149

Structure parameters

• Formula: C78 H71 Cl Ir O2 P4 Rh Si2
• Calculated formula: C78 H71 Cl Ir O2 P4 Rh Si2
• Title of publication: Mixed Bis(μ-silylene) and (μ-Silylene)/(μ-Germylene) Complexes Involving the Rh/Ir Metal Combination: Nature of the Si...Si Interactions in the Bis(μ-silylene) Species
• Authors of publication: Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 9249 - 9258
• a: 20.197 ± 0.0008 Å
• b: 23.1105 ± 0.001 Å
• c: 29.393 ± 0.0012 Å
• α: 90°
• β: 96.3869 ± 0.0005°
• γ: 90°
• Cell volume: 13634.4 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0391
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0712
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No