Information card for entry 4330152

Structure parameters

• Formula: C71 H62 Cl2 Ir O2 P4 Rh Si2
• Calculated formula: C71 H62 Cl2 Ir O2 P4 Rh Si2
• Title of publication: Mixed Bis(μ-silylene) and (μ-Silylene)/(μ-Germylene) Complexes Involving the Rh/Ir Metal Combination: Nature of the Si...Si Interactions in the Bis(μ-silylene) Species
• Authors of publication: Md Hosnay Mobarok; Robert McDonald; Michael J. Ferguson; Martin Cowie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 9249 - 9258
• a: 19.1085 ± 0.0009 Å
• b: 15.2861 ± 0.0007 Å
• c: 21.5289 ± 0.001 Å
• α: 90°
• β: 90.6052 ± 0.0007°
• γ: 90°
• Cell volume: 6288.1 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0479
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0652
• Weighted residual factors for all reflections included in the refinement: 0.072
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No