Information card for entry 4330566

Structure parameters

• Formula: C33 H50 Cl3 F6 N5 P3 Rh
• Calculated formula: C33 H50 Cl3 F6 N5 P3 Rh
• Title of publication: Syntheses and Electronic Properties of Rhodium(III) Complexes Bearing a Redox-Active Ligand
• Authors of publication: Sarath Wanniarachchi; Brendan J. Liddle; Brandon Kizer; Jeewantha S. Hewage; Sergey V. Lindeman; James R. Gardinier
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 10572 - 10580
• a: 21.7617 ± 0.0006 Å
• b: 67.332 ± 0.0019 Å
• c: 10.8818 ± 0.0003 Å
• α: 90°
• β: 91.578 ± 0.001°
• γ: 90°
• Cell volume: 15938.6 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0522
• Weighted residual factors for significantly intense reflections: 0.1445
• Weighted residual factors for all reflections included in the refinement: 0.1695
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No