Information card for entry 4330568

Structure parameters

• Formula: C38.3 H42.37 Cl5 F3 N7 O3 Rh S
• Calculated formula: C38.28 H42.32 Cl5 F3 N7 O3 Rh S
• Title of publication: Syntheses and Electronic Properties of Rhodium(III) Complexes Bearing a Redox-Active Ligand
• Authors of publication: Sarath Wanniarachchi; Brendan J. Liddle; Brandon Kizer; Jeewantha S. Hewage; Sergey V. Lindeman; James R. Gardinier
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 10572 - 10580
• a: 14.9796 ± 0.0004 Å
• b: 32.8756 ± 0.0007 Å
• c: 9.1507 ± 0.0003 Å
• α: 90°
• β: 105.548 ± 0.003°
• γ: 90°
• Cell volume: 4341.5 ± 0.2 ų
• Cell temperature: 99.9 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1414
• Residual factor for significantly intense reflections: 0.1329
• Weighted residual factors for significantly intense reflections: 0.299
• Weighted residual factors for all reflections included in the refinement: 0.3025
• Goodness-of-fit parameter for all reflections included in the refinement: 1.236
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No