Information card for entry 4330704

Structure parameters

• Formula: C52 H59 Cl2 N3 Si2
• Calculated formula: C52 H59 Cl2 N3 Si2
• Title of publication: Stable Silaimines with Three- and Four-Coordinate Silicon Atoms
• Authors of publication: Prinson P. Samuel; Ramachandran Azhakar; Rajendra S. Ghadwal; Sakya S. Sen; Herbert W. Roesky; Markus Granitzka; Julia Matussek; Regine Herbst-Irmer; Dietmar Stalke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 11049 - 11054
• a: 12.102 ± 0.002 Å
• b: 16.373 ± 0.002 Å
• c: 24.055 ± 0.003 Å
• α: 90°
• β: 92.06 ± 0.03°
• γ: 90°
• Cell volume: 4763.3 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0841
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1067
• Weighted residual factors for all reflections included in the refinement: 0.1245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No