Information card for entry 4330967

Structure parameters

• Formula: C24 H60 Na O88 P2 Rb9 Sb4 W18
• Calculated formula: C24 H20 O82.5 P2 Rb9 Sb4 W18
• SMILES: [W]1234(O[Sb](O[W]56(=O)(O1)O[W]178(=O)[O]9%10[W]%11%12(=O)(O1)O[W]1%13%14(O[Sb](O[W](=O)(O3)([O]1=P%10([O]1[W]3(=O)([O]=[Sb]%10(c%15ccccc%15)O[W]%15%16%17(=O)O[W]%18%19(O%10)(=O)O[W]%10%20%21(=O)[O]%22%23[W]%24%25(=O)(O%10)O[W]%10%26%27(O[Sb](c%28ccccc%28)(=[O][W]1(=O)(O8)(O6)O3)O[W](=O)(O%16)([O]%10=P%23([O]1[W](=O)(=O)(O%25)(O%26)O[W]1(=O)(=O)(O%21)O%19)[O]%17%18)(O%27)O[W]%22(=O)(O%15)(O%20)O%24)=O)(O%12)O%13)[O]45)(O%14)O[W]9(=O)(O2)(O7)O%11)c1ccccc1)=O)c1ccccc1)=O.[Rb+].[Rb+].[Rb+].[Rb+].[Rb+].O.O.O.O.O.O.O.O.[Rb+].[Rb+].[Rb+].[Rb+].O.O.O.O.O.O.O
• Title of publication: Synthesis and Biological Activity of Organoantimony(III)-Containing Heteropolytungstates
• Authors of publication: Maria Barsukova-Stuckart; Luis F. Piedra-Garza; Bimersha Gautam; Gabriela Alfaro-Espinoza; Natalya V. Izarova; Abhishek Banerjee; Bassem S. Bassil; Matthias S. Ullrich; Hans J. Breunig; Cristian Silvestru; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 12015 - 12022
• a: 12.7882 ± 0.0016 Å
• b: 13.9014 ± 0.0016 Å
• c: 16.236 ± 0.002 Å
• α: 73.118 ± 0.007°
• β: 77.083 ± 0.008°
• γ: 65.203 ± 0.007°
• Cell volume: 2490 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0621
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for significantly intense reflections: 0.1272
• Weighted residual factors for all reflections included in the refinement: 0.1607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No