Information card for entry 4330994

Structure parameters

• Formula: C45 H55 Cl4 I2 N4 Rh
• Calculated formula: C45 H55 Cl4 I2 N4 Rh
• Title of publication: Ligand Effects on the Oxidative Addition of Halogens to (dpp-nacnacR)Rh(phdi)
• Authors of publication: David W. Shaffer; Scott A. Ryken; Ryan A. Zarkesh; Alan F. Heyduk
• Journal of publication: Inorganic Chemistry
• Year of publication: 2012
• Journal volume: 51
• Pages of publication: 12122 - 12131
• a: 11.72 ± 0.0014 Å
• b: 20 ± 0.002 Å
• c: 20.356 ± 0.002 Å
• α: 90°
• β: 100.673 ± 0.002°
• γ: 90°
• Cell volume: 4688.9 ± 0.9 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for significantly intense reflections: 0.0628
• Weighted residual factors for all reflections included in the refinement: 0.0685
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No