Crystallography Open Database

Information card for entry 4331098

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Coordinates	4331098.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C184 H292 Co10.52 N14 Ni9.48 O77
Calculated formula	C184 H220 Co10.52 N14 Ni9.48 O77
Title of publication	Wheel-Shaped Icosanuclear Homo- and Heterometallic Complexes of NiII, CoII, and CuII Ions Supported by Unsymmetrical Aminoalcohol Ligands
Authors of publication	Takayuki Nakajima; Keiko Seto; Fumihiro Horikawa; Isao Shimizu; Andreas Scheurer; Bunsho Kure; Takashi Kajiwara; Tomoaki Tanase; Masahiro Mikuriya
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	12503 - 12510
a	22.724 ± 0.011 Å
b	22.724 ± 0.011 Å
c	22.778 ± 0.012 Å
α	90°
β	90°
γ	90°
Cell volume	11762 ± 10 Å³
Cell temperature	153 K
Ambient diffraction temperature	153 K
Number of distinct elements	6
Space group number	86
Hermann-Mauguin space group symbol	P 42/n :2
Hall space group symbol	-P 4bc
Residual factor for significantly intense reflections	0.0664
Weighted residual factors for all reflections included in the refinement	0.2065
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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