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Information card for entry 4331284
Preview
Coordinates | 4331284.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C72 H122 K N4 Ni2 O8 |
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Calculated formula | C72 H122 K N4 Ni2 O8 |
SMILES | C1(C(C)=[N]([Ni]23([H][Ni]43([N](=C(C(C)=[N]4c3c(cccc3C(C)C)C(C)C)C)c3c(cccc3C(C)C)C(C)C)[H]2)[N]=1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C)C.[K]1234([O](C)CC[O]1C)([O](C)CC[O]2C)([O](C)CC[O]3C)[O](C)CC[O]4C |
Title of publication | Synthesis and Reactivity of Nickel Hydride Complexes of an α-Diimine Ligand |
Authors of publication | Qingsong Dong; Yanxia Zhao; Yuanting Su; Ji-Hu Su; Biao Wu; Xiao-Juan Yang |
Journal of publication | Inorganic Chemistry |
Year of publication | 2012 |
Journal volume | 51 |
Pages of publication | 13162 - 13170 |
a | 13.2561 ± 0.0013 Å |
b | 36.709 ± 0.004 Å |
c | 17.7651 ± 0.0017 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 8644.8 ± 1.5 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 60 |
Hermann-Mauguin space group symbol | P b c n |
Hall space group symbol | -P 2n 2ab |
Residual factor for all reflections | 0.1167 |
Residual factor for significantly intense reflections | 0.0756 |
Weighted residual factors for significantly intense reflections | 0.1973 |
Weighted residual factors for all reflections included in the refinement | 0.2168 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.126 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4331284.html
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Users of the data should acknowledge the original authors of the
structural data.