Information card for entry 4331486

Structure parameters

• Common name: Cs4Pb4Ge5S16
• Formula: Cs4 Ge5 Pb4 S16
• Calculated formula: Cs4 Ge5 Pb4 S16
• Title of publication: Exploratory Synthesis in Molten Salts: Role of Flux Basicity in the Stabilization of the Complex Thiogermanates Cs4Pb4Ge5S16, K2PbGe2S6, and K4Sn3Ge3S14
• Authors of publication: Palchik, Oleg; Marking, Gregory M.; Kanatzidis, Mercouri G.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Journal issue: 12
• Pages of publication: 4151 - 4153
• a: 38.302 ± 0.0019 Å
• b: 9.077 ± 0.0005 Å
• c: 19.4421 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6759.4 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 64
• Hermann-Mauguin space group symbol: C m c a
• Hall space group symbol: -C 2ac 2
• Residual factor for all reflections: 0.0416
• Residual factor for significantly intense reflections: 0.0249
• Weighted residual factors for significantly intense reflections: 0.0584
• Weighted residual factors for all reflections included in the refinement: 0.0636
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No