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Information card for entry 4331503
Preview
Coordinates | 4331503.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H43 O S Sm |
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Calculated formula | C30 H43 O S Sm |
Title of publication | Synthesis, Structure, and Ligand-Based Reduction Reactivity of Trivalent Organosamarium Benzene Chalcogenolate Complexes (C5Me5)2Sm(EPh)(THF) and [(C5Me5)2Sm(μ-EPh)]2 |
Authors of publication | Evans, William J.; Miller, Kevin A.; Lee, David S.; Ziller, Joseph W. |
Journal of publication | Inorganic Chemistry |
Year of publication | 2005 |
Journal volume | 44 |
Journal issue | 12 |
Pages of publication | 4326 - 4332 |
a | 17.5355 ± 0.0006 Å |
b | 15.1031 ± 0.0005 Å |
c | 21.2702 ± 0.0007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5633.2 ± 0.3 Å3 |
Cell temperature | 163 ± 2 K |
Ambient diffraction temperature | 163 ± 2 K |
Number of distinct elements | 5 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0837 |
Residual factor for significantly intense reflections | 0.04 |
Weighted residual factors for significantly intense reflections | 0.0798 |
Weighted residual factors for all reflections included in the refinement | 0.0977 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.029 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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