Information card for entry 4331540
| Formula |
C156 H158 F48 N38 O6 P8 Pd8 |
| Calculated formula |
C156 H158 F48 N38 O6 P8 Pd8 |
| Title of publication |
Solution self-assembly, spontaneous deprotonation, and crystal structures of bipyrazolate-bridged metallomacrocycles with dimetal centers. |
| Authors of publication |
Yu, Shu-Yan; Huang, Hai-Ping; Li, Sheng-Hui; Jiao, Qing; Li, Yi-Zhi; Wu, Biao; Sei, Yoshihisa; Yamaguchi, Kentaro; Pan, Yuan-Jiang; Ma, Hong-Wei |
| Journal of publication |
Inorganic chemistry |
| Year of publication |
2005 |
| Journal volume |
44 |
| Journal issue |
25 |
| Pages of publication |
9471 - 9488 |
| a |
12.454 ± 0.002 Å |
| b |
22.437 ± 0.004 Å |
| c |
27.684 ± 0.005 Å |
| α |
77.492 ± 0.004° |
| β |
78.918 ± 0.004° |
| γ |
82.733 ± 0.004° |
| Cell volume |
7382 ± 2 Å3 |
| Cell temperature |
293 ± 2 K |
| Ambient diffraction temperature |
293 ± 2 K |
| Number of distinct elements |
7 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0958 |
| Residual factor for significantly intense reflections |
0.0639 |
| Weighted residual factors for significantly intense reflections |
0.1575 |
| Weighted residual factors for all reflections included in the refinement |
0.166 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.046 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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https://www.crystallography.net/4331540.html
