Information card for entry 4331596

Structure parameters

• Formula: C26 H43 B Ni O2 P2
• Calculated formula: C26 H43 B Ni O2 P2
• Title of publication: Pincer-Ligated Nickel Hydridoborate Complexes: the Dormant Species in Catalytic Reduction of Carbon Dioxide with Boranes
• Authors of publication: Sumit Chakraborty; Jie Zhang; Yogi J. Patel; Jeanette A. Krause; Hairong Guan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 37 - 47
• a: 8.7254 ± 0.0001 Å
• b: 10.506 ± 0.0002 Å
• c: 14.5596 ± 0.0002 Å
• α: 81.742 ± 0.001°
• β: 86.572 ± 0.001°
• γ: 83.28 ± 0.001°
• Cell volume: 1310.5 ± 0.03 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.0999
• Weighted residual factors for all reflections included in the refinement: 0.1043
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No