Synthesis, Structural and Spectroscopic Characterization, Catalytic Properties, and Thermal Transformations of New Cyclic Di- and Trisiloxanediolato Tantalum Complexes
Authors of publication
Kapoor, Ramesh N.; Cervantes-Lee, Francisco; Campana, Charles F.; Haltiwanger, Curtis; Abney, Kent; Pannell, Keith H.
Journal of publication
Inorganic Chemistry
Year of publication
2006
Journal volume
45
Journal issue
5
Pages of publication
2203 - 2208
a
9.2043 ± 0.0008 Å
b
10.7671 ± 0.001 Å
c
11.8911 ± 0.0011 Å
α
103.649 ± 0.002°
β
111.626 ± 0.002°
γ
105.234 ± 0.002°
Cell volume
981.55 ± 0.16 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0451
Residual factor for significantly intense reflections
0.0378
Weighted residual factors for significantly intense reflections
0.0933
Weighted residual factors for all reflections included in the refinement
0.0992
Goodness-of-fit parameter for all reflections included in the refinement
