Information card for entry 4331630

Structure parameters

• Formula: C88 H63 Mo N6 O4 P4
• Calculated formula: C88 H63 Mo N6 O4 P4
• Title of publication: Preparation, Characterization, and Reactivity of Dinitrogen Molybdenum Complexes with Bis(diphenylphosphino)amine Derivative Ligands that Form a Unique 4-Membered P-N-P Chelate Ring
• Authors of publication: Takahiko Ogawa; Yuji Kajita; Yuko Wasada-Tsutsui; Hiroaki Wasada; Hideki Masuda
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 182 - 195
• a: 11.273 ± 0.004 Å
• b: 18.535 ± 0.006 Å
• c: 20.253 ± 0.007 Å
• α: 95.201 ± 0.005°
• β: 94.064 ± 0.004°
• γ: 102.522 ± 0.005°
• Cell volume: 4096 ± 2 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0737
• Weighted residual factors for all reflections included in the refinement: 0.2261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No