Information card for entry 4331634

Structure parameters

• Formula: C70 H58 Cl2 Mo N2 O1.5 P4
• Calculated formula: C70 H58 Cl2 Mo N2 O1.5 P4
• Title of publication: Preparation, Characterization, and Reactivity of Dinitrogen Molybdenum Complexes with Bis(diphenylphosphino)amine Derivative Ligands that Form a Unique 4-Membered P-N-P Chelate Ring
• Authors of publication: Takahiko Ogawa; Yuji Kajita; Yuko Wasada-Tsutsui; Hiroaki Wasada; Hideki Masuda
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 182 - 195
• a: 18.6171 ± 0.0003 Å
• b: 11.351 ± 0.0002 Å
• c: 30.2636 ± 0.0007 Å
• α: 90°
• β: 101.856 ± 0.0009°
• γ: 90°
• Cell volume: 6258.9 ± 0.2 ų
• Cell temperature: 173.1 K
• Ambient diffraction temperature: 173.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for all reflections included in the refinement: 0.1193
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No