Information card for entry 4332044

Structure parameters

• Formula: C31.5 H50 K N O6 Si2
• Calculated formula: C31.5 H46 K N O6 Si2
• Title of publication: Lanthanum and Alkali Metal Coordination Chemistry of the Bis(dimethylphenylsilyl)amide Ligand
• Authors of publication: Evans, William J.; Rego, Daniel B.; Ziller, Joseph W.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 8
• Pages of publication: 3437 - 3443
• a: 11.6717 ± 0.0014 Å
• b: 11.7444 ± 0.0014 Å
• c: 13.7456 ± 0.0017 Å
• α: 87.787 ± 0.002°
• β: 76.661 ± 0.002°
• γ: 72.868 ± 0.002°
• Cell volume: 1751.2 ± 0.4 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1943
• Residual factor for significantly intense reflections: 0.148
• Weighted residual factors for significantly intense reflections: 0.3652
• Weighted residual factors for all reflections included in the refinement: 0.4101
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No