Information card for entry 4332152

Structure parameters

• Formula: C19 H22 O5 W
• Calculated formula: C19 H22 O5 W
• Title of publication: Bis(acetylacetonato)tricarbonyl Tungsten(II): A Convenient Precursor to Chiral Bis(acac) Tungsten(II) Complexes
• Authors of publication: Jackson, Andrew B.; White, Peter S.; Templeton, Joseph L.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 16
• Pages of publication: 6205 - 6213
• a: 8.4393 ± 0.0004 Å
• b: 20.2238 ± 0.001 Å
• c: 11.1917 ± 0.0004 Å
• α: 90°
• β: 106.649 ± 0.003°
• γ: 90°
• Cell volume: 1830.06 ± 0.14 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.044
• Residual factor for significantly intense reflections: 0.032
• Weighted residual factors for all reflections: 0.141
• Weighted residual factors for significantly intense reflections: 0.039
• Goodness-of-fit parameter for significantly intense reflections: 1.31
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No