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Information card for entry 4332310
Preview
Coordinates | 4332310.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | TpOs(cod)OMe*MeOH |
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Formula | C19 H29 B N6 O2 Os |
Calculated formula | C19 H29 B N6 O2 Os |
SMILES | [Os]12345([n]6n([BH](n7[n]1ccc7)n1[n]2ccc1)ccc6)([CH]1=[CH]3CC[CH]4=[CH]5CC1)OC.CO |
Title of publication | Synthesis and Characterization of Osmium(II) Trispyrazolylborate Complexes |
Authors of publication | Dickinson, Paul W.; Girolami, Gregory S. |
Journal of publication | Inorganic Chemistry |
Year of publication | 2006 |
Journal volume | 45 |
Journal issue | 13 |
Pages of publication | 5215 - 5224 |
a | 10.7281 ± 0.0014 Å |
b | 14.0044 ± 0.0019 Å |
c | 13.9058 ± 0.0018 Å |
α | 90° |
β | 102.418 ± 0.002° |
γ | 90° |
Cell volume | 2040.3 ± 0.5 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0359 |
Residual factor for significantly intense reflections | 0.0247 |
Weighted residual factors for significantly intense reflections | 0.0513 |
Weighted residual factors for all reflections included in the refinement | 0.0539 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.96 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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