Information card for entry 4332407

Structure parameters

• Formula: C24 H36 Ge8 N8 Pb8
• Calculated formula: C24 H18 Ge8 N8 Pb8
• Title of publication: Synthesis and Characterization of Imidocubanes with Exocube GeIVand SnIVSubstituents: [M(μ3-NGeMe3)]4(M = Sn, Ge, Pb); [Sn(μ3-NSnMe3)]4
• Authors of publication: Eichler, Jack F.; Just, Oliver; Rees, William S.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 17
• Pages of publication: 6706 - 6712
• a: 18.2282 ± 0.0014 Å
• b: 18.2282 ± 0.0014 Å
• c: 18.2282 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6056.6 ± 0.8 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 218
• Hermann-Mauguin space group symbol: P -4 3 n
• Hall space group symbol: P -4n 2 3
• Residual factor for all reflections: 0.1119
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1417
• Weighted residual factors for all reflections included in the refinement: 0.1753
• Goodness-of-fit parameter for all reflections included in the refinement: 0.974
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No