Crystallography Open Database

Information card for entry 4332699

Preview

Coordinates	4332699.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H52 Cl2 O3.5 P2 Rh2
Calculated formula	C40 H52 Cl2 O3.5 P2 Rh2
Title of publication	Roof-Shaped Halide-Bridged Bimetallic Complexes via Ring Expansion Reaction
Authors of publication	Azerraf, Clarite; Cohen, Shmuel; Gelman, Dmitri
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	17
Pages of publication	7010 - 7017
a	12.9612 ± 0.0008 Å
b	13.7251 ± 0.0008 Å
c	15.1256 ± 0.0009 Å
α	83.692 ± 0.001°
β	66.619 ± 0.001°
γ	62.343 ± 0.001°
Cell volume	2178.4 ± 0.2 Å³
Cell temperature	295 ± 2 K
Ambient diffraction temperature	295 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0548
Residual factor for significantly intense reflections	0.0375
Weighted residual factors for significantly intense reflections	0.0939
Weighted residual factors for all reflections included in the refinement	0.0975
Goodness-of-fit parameter for all reflections included in the refinement	0.933
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4332699.html