Information card for entry 4332802

Structure parameters

• Formula: C64 H116 Mo12 N8 O60 P
• Calculated formula: C64 H108 Mo12 N8 O60 P
• Title of publication: Formation ofp-Phenylenediamine−Crown Ether−[PMo12O40]4-Salts
• Authors of publication: Akutagawa, Tomoyuki; Endo, Daigoro; Imai, Hiroyuki; Noro, Shin-ichiro; Cronin, Leroy; Nakamura, Takayoshi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 21
• Pages of publication: 8628 - 8637
• a: 13.74 ± 0.03 Å
• b: 14.52 ± 0.02 Å
• c: 16.26 ± 0.03 Å
• α: 65.13 ± 0.06°
• β: 64.74 ± 0.06°
• γ: 67.12 ± 0.06°
• Cell volume: 2574 ± 8 ų
• Cell temperature: 296.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0434
• Weighted residual factors for all reflections included in the refinement: 0.0646
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No