Information card for entry 4333140

Structure parameters

• Formula: C40 H60 Ce2 O
• Calculated formula: C40 H60 Ce2 O
• Title of publication: Synthesis, Structure, and15N NMR Studies of Paramagnetic Lanthanide Complexes Obtained by Reduction of Dinitrogen
• Authors of publication: Evans, William J.; Rego, Daniel B.; Ziller, Joseph W.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 26
• Pages of publication: 10790 - 10798
• a: 11.4716 ± 0.0006 Å
• b: 11.4716 ± 0.0006 Å
• c: 14.2381 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1873.7 ± 0.2 ų
• Cell temperature: 163 ± 2 K
• Ambient diffraction temperature: 163 ± 2 K
• Number of distinct elements: 4
• Space group number: 121
• Hermann-Mauguin space group symbol: I -4 2 m
• Hall space group symbol: I -4 2
• Residual factor for all reflections: 0.0198
• Residual factor for significantly intense reflections: 0.017
• Weighted residual factors for significantly intense reflections: 0.0402
• Weighted residual factors for all reflections included in the refinement: 0.0417
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No