Information card for entry 4333150

Structure parameters

• Formula: C16 H52 Fe2 N12 Sb4 Se9
• Calculated formula: C16 H45 Fe2 N12 Sb4 Se9
• Title of publication: Mixed-Valent Selenidoantimonates(III,V) with Transition-Metal Complexes as Counterions: Solvothermal Syntheses and Characterization of [M(dien)2]2Sb4Se9(M = Mn, Fe), [Co(dien)2]2Sb2Se6, and [Ni(dien)2]2Sb2Se5
• Authors of publication: Jia, Dingxian; Zhang, Yong; Zhao, Qianxin; Deng, Jie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2006
• Journal volume: 45
• Journal issue: 24
• Pages of publication: 9812 - 9817
• a: 11.8107 ± 0.0008 Å
• b: 11.6077 ± 0.0008 Å
• c: 31.955 ± 0.002 Å
• α: 90°
• β: 95.42 ± 0.002°
• γ: 90°
• Cell volume: 4361.3 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0622
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.0978
• Weighted residual factors for all reflections included in the refinement: 0.1032
• Goodness-of-fit parameter for all reflections included in the refinement: 1.149
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No