Information card for entry 4333215

Structure parameters

• Formula: C13 H33 Br N4 Si W
• Calculated formula: C13 H33 Br N4 Si W
• Title of publication: Volatile Imido−Hydrazido Compounds of the Refractory Metals Niobium, Tantalum, Molybdenum, and Tungsten
• Authors of publication: Gaess, Daniel; Harms, Klaus; Pokoj, Michael; Stolz, Wolfgang; Sundermeyer, Jörg
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 16
• Pages of publication: 6688 - 6701
• a: 14.8943 ± 0.0012 Å
• b: 10.2528 ± 0.0005 Å
• c: 14.6359 ± 0.0012 Å
• α: 90°
• β: 100.874 ± 0.007°
• γ: 90°
• Cell volume: 2194.9 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0282
• Residual factor for significantly intense reflections: 0.0208
• Weighted residual factors for significantly intense reflections: 0.0458
• Weighted residual factors for all reflections included in the refinement: 0.0472
• Goodness-of-fit parameter for all reflections included in the refinement: 0.963
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No