Information card for entry 4333222

Structure parameters

• Formula: C42 H74 N4 Os P4 S4
• Calculated formula: C42 H57 N4 Os P4 S4
• Title of publication: Synthesis, crystal structures, and reactivity of osmium(II) and -(IV) complexes containing a dithioimidodiphosphinate ligand.
• Authors of publication: Cheung, Wai-Man; Zhang, Qian-Feng; Williams, Ian D.; Leung, Wa-Hung
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 14
• Pages of publication: 5754 - 5762
• a: 12.5973 ± 0.0012 Å
• b: 12.7653 ± 0.0012 Å
• c: 17.1029 ± 0.0017 Å
• α: 102.619 ± 0.002°
• β: 98.489 ± 0.002°
• γ: 100.346 ± 0.002°
• Cell volume: 2589.7 ± 0.4 ų
• Cell temperature: 250 ± 2 K
• Ambient diffraction temperature: 250 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.0338
• Weighted residual factors for significantly intense reflections: 0.0814
• Weighted residual factors for all reflections included in the refinement: 0.0852
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No