Information card for entry 4333253

Structure parameters

• Formula: C33 H35 Cl2 N O3 P Re
• Calculated formula: C33 H35 Cl2 N O3 P Re
• Title of publication: Rhenium(V) oxo complexes with acetylacetone derived Schiff bases: structure and catalytic epoxidation.
• Authors of publication: Sachse, Anna; Mösch-Zanetti, Nadia C; Lyashenko, Ganna; Wielandt, J. Wolfram; Most, Kerstin; Magull, Jörg; Dall'Antonia, Fabio; Pal, Aritra; Herbst-Irmer, Regine
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 7129 - 7135
• a: 9.048 ± 0.003 Å
• b: 21.65 ± 0.003 Å
• c: 15.583 ± 0.003 Å
• α: 90°
• β: 91.75 ± 0.03°
• γ: 90°
• Cell volume: 3051.1 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0197
• Residual factor for significantly intense reflections: 0.0175
• Weighted residual factors for significantly intense reflections: 0.0424
• Weighted residual factors for all reflections included in the refinement: 0.0433
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No