Information card for entry 4333301

Structure parameters

• Formula: C32 H118 As16 N24 O87 V24 Zn8
• Calculated formula: C32 H100 As16 N24 O87 V24 Zn8
• Title of publication: In situ ligand reactions under hydrothermal conditions afford a novel zinc-substituted polyoxovanadate dimer.
• Authors of publication: Zheng, Shou-Tian; Wang, Ming-Hui; Yang, Guo-Yu
• Journal of publication: Inorganic chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 22
• Pages of publication: 9503 - 9508
• a: 15.5635 ± 0.0003 Å
• b: 19.6903 ± 0.0004 Å
• c: 24.8067 ± 0.0004 Å
• α: 85.215 ± 0.005°
• β: 89.402 ± 0.004°
• γ: 82.088 ± 0.003°
• Cell volume: 7503.4 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1333
• Residual factor for significantly intense reflections: 0.0893
• Weighted residual factors for significantly intense reflections: 0.2164
• Weighted residual factors for all reflections included in the refinement: 0.2504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No