Information card for entry 4333468

Structure parameters

• Formula: C48 H38 As Cu3 Mo12 N8 O43 V2
• Calculated formula: C48 H40 As Cu3 Mo12 N8 O44 V2
• Title of publication: Asymmetrical Polar Modification of a Bivanadium-Capped Keggin POM by Multiple Cu−N Coordination Polymeric Chains
• Authors of publication: Sha, Jing-quan; Peng, Jun; Liu, Hong-sheng; Chen, Jing; Tian, Ai-xiang; Zhang, Peng-peng
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Journal issue: 26
• Pages of publication: 11183 - 11189
• a: 12.274 ± 0.004 Å
• b: 12.872 ± 0.004 Å
• c: 13.108 ± 0.004 Å
• α: 93.971 ± 0.005°
• β: 104.876 ± 0.004°
• γ: 110.758 ± 0.005°
• Cell volume: 1842 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1287
• Residual factor for significantly intense reflections: 0.0781
• Weighted residual factors for significantly intense reflections: 0.1733
• Weighted residual factors for all reflections included in the refinement: 0.1998
• Goodness-of-fit parameter for all reflections included in the refinement: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No