Information card for entry 4333500

Structure parameters

• Formula: C35 H36 Cl4 N4 Os P2
• Calculated formula: C35 H36 Cl4 N4 Os P2
• SMILES: [Os]12(Cl)([P](CCn3[n]1ccc3)(c1ccccc1)c1ccccc1)(Cl)[P](CCn1[n]2ccc1)(c1ccccc1)c1ccccc1.ClCCl
• Title of publication: Ru and Os Complexes Containing a P,N-Donor Heterotopic Ligand: The Effect of Solvent on Stereochemistry
• Authors of publication: Dabb, Serin L.; Messerle, Barbara A.; Smith, Matthew K.; Willis, Anthony C.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Journal issue: 8
• Pages of publication: 3034 - 3044
• a: 10.25 ± 0.002 Å
• b: 19.019 ± 0.004 Å
• c: 37.938 ± 0.008 Å
• α: 90°
• β: 92.48 ± 0.03°
• γ: 90°
• Cell volume: 7389 ± 3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1025
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1156
• Weighted residual factors for all reflections included in the refinement: 0.1254
• Goodness-of-fit parameter for all reflections included in the refinement: 1.23
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 4304396
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No