Information card for entry 4333709

Structure parameters

• Formula: C21 H46 B2 Li O4 P Si2
• Calculated formula: C21 H46 B2 Li O4 P Si2
• Title of publication: Phosphido-Borane and Phosphido-Bis(Borane) Complexes of the Alkali Metals, a Comparative Study
• Authors of publication: Keith Izod; James M. Watson; William Clegg; Ross W. Harrington
• Journal of publication: Inorganic Chemistry
• Year of publication: 2013
• Journal volume: 52
• Pages of publication: 1466 - 1475
• a: 15.028 ± 0.0003 Å
• b: 12.7789 ± 0.0003 Å
• c: 14.9822 ± 0.0003 Å
• α: 90°
• β: 92.8258 ± 0.0017°
• γ: 90°
• Cell volume: 2873.7 ± 0.11 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0739
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1893
• Weighted residual factors for all reflections included in the refinement: 0.1958
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No