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Information card for entry 4333814
Preview
Coordinates | 4333814.cif |
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Original paper (by DOI) | HTML |
Chemical name | Bis{1-tert-butanolato-(2,9,10-trioxa-6-aza-8,8,11,11- tetramethylstannatricyclo-[4.3.3.0^1.6^]dodecane} toluene solvate |
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Formula | C37 H70 N2 O8 Sn2 |
Calculated formula | C37 H70 N2 O8 Sn2 |
Title of publication | Novel Trialkanolamine Derivatives of Tin of the Type [N(CH2CMe2O)2(CH2)nOSnOR]m (m= 1, 2;n= 2, 3; R =t-Bu, 2,6-Me2C6H3) and Related Tri- and Pentanuclear Tin(IV) Oxoclusters. Syntheses and Molecular Structures |
Authors of publication | Thomas Zöller; Klaus Jurkschat |
Journal of publication | Inorganic Chemistry |
Year of publication | 2013 |
Journal volume | 52 |
Pages of publication | 1872 - 1882 |
a | 11.8063 ± 0.0006 Å |
b | 12.5549 ± 0.0006 Å |
c | 14.1181 ± 0.0008 Å |
α | 90° |
β | 102.23 ± 0.006° |
γ | 90° |
Cell volume | 2045.19 ± 0.19 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0386 |
Residual factor for significantly intense reflections | 0.0258 |
Weighted residual factors for significantly intense reflections | 0.0488 |
Weighted residual factors for all reflections included in the refinement | 0.0499 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.89 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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